XRD, DSC and Raman studies of phases transition in NH3(CH2)6NH3BiCl5
978-3-330-03274-3
333003274X
64
2017-01-27
28,90 €
eng
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The hexylenediammonium pentachlorobismuthate, NH3(CH2)6NH3BiCl5 crystal has been studied by means of XRD, DSC and spectroscopy (IR and Raman)techniques. The X-ray powder study develooped at different temperatures showed that the crystal exhibits two phase transitions near 286 K and 326 K. The DSC analysis (on heating and couling) confirmed the existence of these phase transitions at 291/286 K and 326/325 K. The Raman spectroscopy study made at various temperatures showed that both anionic and cationic motions contribute to the complex transition mechanisms.
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Chimica inorganica
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